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Structure Determination by X-ray Crystallography
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概要 | X-ray crystallography provides us with the most accurate picture we can get of atomic and molecular structures in crystals. It provides a hard bedrock of structural results in chemistry and in mineral...ogy. In biology, where the structures are not fully crystalline, it can still provide valuable results and, indeed, the impact here has been revolutionary. It is still an immense field for young workers, and no doubt will provide yet more striking developments of a major character. It does, however, require a wide range of intellectual application, and a considerable ability in many fields. This book will provide much help. It is a very straightforward and thorough guide to every aspect of the subject. The authors are ex perienced both as research workers and as teachers of standing, and this is shown in their clarity of exposition. There are plenty of illustrations and worked examples to aid the student to obtain a real grasp of the subject. The practical side is encouraged by the very clarity of the theory.続きを見る |
目次 | 1 Crystal Geometry.I 2 Crystal Geometry. II 3 Preliminary Examination of Crystals by Optical and X-ray Methods 4 Scattering of X-rays by Crystals 5 Fourier Transform Theory 6 Techniques in X-ray Structure Determination 7 Direct Methods and Refinement 8 Examples of Crystal Structure Determination A1 Stereoviews and Crystal Models A1.1 Stereoviews A1.2 Model of a Tetragonal Crystal A2 Crystallographic Point-Group Study and Recognition Scheme A3 Schoenflies' Symmetry Notation A3.1 Alternating Axis of Symmetry A3.2 Notation A4 Generation and Properties of X-rays A4.1 X-rays and White Radiation A4.2 Characteristic X-rays A4.3 Absorption of X-rays A4.4 Filtered Radiation A5 Crystal Perfection and Intensity Measurement A5.1 Crystal Perfection A5.2 Intensity of Reflected Beam A5.3 Intensity Measurements on Photographs A5.4 Data Processing A5.4.1 Introduction A5.4.2 Standard Deviation of Intensity A5.4.3 Absorption Corrections A5.4.4 Scaling A5.4.5 Merging Equivalent Reflections A6 Transformations A7 Comments on Some Orthorhombic and Monoclinic Space Groups A7.1 Orthorhombic Space Groups A7.2 Monoclinic Space Groups A8 Vector Algebraic Relationships in Reciprocal Space A8.1 Introduction A8.2 Reciprocal Lattice A8.2.1 Interplanar Spacings A8.2.2 Volume of a Parallelepipedon A8.2.3 Reciprocity of Unit-Cell Volumes A8.2.4 Angle between Bravais Lattice Planes A8.2.5 Reciprocity of F and I Unit Cells A8.3 X-ray Diffraction and the Reciprocal Lattice A8.3.1 Bragg's Equation A8.4 Crystal Setting A8.4.1 Setting Technique A9 Intensity Statistics A9.1 Weighted Reciprocal Lattice A9.1.1 Laue Symmetry A9.1.2 Systematic Absences A9.1.3 Accidental Absences A9.1.4 Enhanced Averages A9.1.5 Special Distributions A10 Enantiomorph Selection A11 Analytical Geometry of Direction Cosines A11.1 Direction Cosines of a Line A11.2 Angle between Two Lines A12 The Stereographic Projection of a Circle Is a Circle A13 Setting a Crystal for Precession Photography A13.1 Setting a Crystal Axis Parallel to the X-ray Beam A13.2 Setting a Reciprocal Lattice Row Horizontally A13.3 Screen Setting A14 Synchrotron Radiation Solutions.続きを見る |
本文を見る | Full text available from SpringerLink ebooks - Physics and Astronomy (Archive) |
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登録日 | 2020.06.27 |
更新日 | 2020.06.28 |